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The analysis was performed on HPLC, and the conditions included 65% of mobile phase A (10 mM ammonium acetate, pH 5 adjusted with 2% acetic acid) and 35% mobile phase B (acetonitrile) in an isocratic elution method
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During the procedure some people may feel some discomfort with sensations of pulling, pinching, tugging, tingling, and cold
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